The numerical value as established in ASTM D3173 or D7582 is used for converting the asdetermined data to a dry basis. • Dry, ashfree basis (daf): The basis for data calculated to a theoretical basis of no moisture or ash associated with the sample. Numerical values as established by ASTM D3173 and D3174, or D7582, are used for converting ...
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The general coal sampling procedures must include these procedures: Get the basic information of the coal including the source of coal (like China coal, India coal), the coal amount and the nominal top size. Ensuring the text parameters and the testsample type; Determining the sampling method is continuous sampling or the intermittent sampling ...
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by heating an airdried coal sample at 105 ... (Btu/lb dry) OF THE INDIANA DANVILLE COAL Source: M. Mastalerz, A Drobniak, J. Rupp and N. Shaffer, "Assessment of the Quality of Indiana coal for Integrated Gasification Combined Cycle Performance (IGCC)', Indiana Geological Survey, Indiana University, June 2005
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In this method, g of airdried coal sample of size 212 µ was taken, pressed to a pellet, and introduced in the bomb. Then it was fired with oxygen, and the result of airdried GCV was recorded. The results of GCV for raw and treated coals were presented in Table 1. (C) Inherent moisture
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Alteration measurements were made in air and in vacuum. A sample of fresh Goonyella coal (10mm, floated to % ash adb) was oxidised by boiling in 30% H 2 O 2 at 100°C for an hour. Figure 1 shows the fluorescence spectra of fresh and treated coal. There is a large decrease in fluorescence intensity.
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(5 marks) 6 (b) gm of air dried coal sample was taken in a crucible, after heating it in an electric oven at 110°C for 1 hr the residue was weighed gm. The residue was heated in Silica crucible covered with vented lid at a temperature 925±257°C for exactly 7 minutes. After cooling the weight of residue was found to contain gm.
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The coal is first finely ground and airdried. Samples of the dried coal are then subjected to several operations, with the sample weights being recorded before and after each operation. Moisture content is determined as the weight loss when a sample is held at 105∘C in an oxygenfree
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The normal preparation procedure requires that each airdried coal sample pass through a jaw crusher; one subsample (split) of the crushed material (2 to 4 mm, or 5 to 10 mesh) is then taken for the ultimate and proximate analyses, and another split is reduced to approximately 150 m m (100 mesh) by a vertical grinder for chemical analysis.
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Drying in air (two stage) airdrying followed by ovendr ying a. Stage I: special moisture sample of I kg of coal crushed (1 mm). weigh the sampl e and the
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About 1 gm of powdered, air dried coal sample is heated in silica crucible at 100 to 105 °C for one hour. Percentage of moisture can be calculated from the loss in weight of the coal sample as
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T 2 distribution and accumulated integral area of pores with different pore sizes for saturated coal after 8 h of drying. Note: sample number 11Rc indicates the test result of the first sample in the first experimental group under raw coal conditions. 11ad8 h is the test result of the first sample in the first experimental group after drying for 8 h in the air environment after saturation.
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Experimental Procedure : About 1g of finely pulverized 212 micron (BSS) airdried coal sample is weighed in a silica crucible and then placed within an electric hot air oven. It is maintained at 110o C. The crucible with the coal sample is allowed to put in the oven for hours and it is taken out with the help of tongues, and then cooled in ...
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Analysis sample of about 300 g of airdried coal, ground to p ass 21 2micron IS Sieve; and in addition special moisture sample of 1 kg of coal, crus hed to pass IS Sieve 125 mm, to be sent in ...
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gm of air dried coal sample was taken in a silica crucible, after heating it in an electric oven at 1050∘C − 1100∘C 1050 ∘ C − 1100 ∘ C for 1 hour, the residue was weighed gm. The residue was heated in silica crucible covered with vented lid at temperature 950 − 9700∘C 950 − 9700 ∘ C for exactly 7 minutes.
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To keep the energy consumption per unit mass of coal dried by hot air the same as that for microwave dried sample, 80 g of the sample with three different kinds of particle sizes was also placed in a drying chamber and the temperature of the drying chamber was kept at 105 °C with a power of kW. Moisture loss was measured by taking out and ...
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Experimental system Thermal analysis. The thermal analysis experiment used a STA449C synchronous thermal analyzer. The initial temperature of the experiment was 30 °C; the heating rate was 10 °C/min; the termination temperature was 800 °C; and the mass of coal samples at different immersion times and airdrying times was 25 ± 1 mg.
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For the analysis of volatile matter in coal, each sample of 1 gram of airdried coal (ground to pass through a 212 microns IS sieve) was taken into a crucible with a lid and placed in the muffle furnace, which was already at a temperature of 9000c for a period of 7 minutes. Then the differences in the weight loss were calculated before and ...
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ADM is Air Dried Moisture (Moisture in the Analysis Sample) NM is Nominated Moisture AR is As Received Basis AD is As Determined (Air Dried) Basis ... Two stage total moisture determination is used when the coal sample is too small mass or too wet to divide or crush without the potential of losing significant amounts of moisture. TMar, % = [Rm ...
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The physical and chemical properties of the airdried residual coal after soaking in the goaf will change, resulting in an increase in its spontaneous combustion tendency. This study aimed to look into the features and mechanism of soakeddried coal's spontaneous combustion. Five samples of coal were dried to various degrees, and the weight loss features during thermal processing were examined ...
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At this time, the hightemperature oxidized coal sample in the goaf experienced water immersion and airdrying, and its surface pore structure changed greatly (As shown in Fig. 1). Therefore, the change in oxygen concentration caused by the strength of air leakage under the development of coal and rock mass fissures, and the ratio of coal ...
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The water content of coal is determined by the industrial analysis of coal. Water is the water of air drying coal samples (Mad). A certain number of coal samples is preairdried into airdried coal samples for laboratory use, which are dried to a constant weight at 102105℃, make the coal sample
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After airdrying, capillary agglomeration decreases, resulting in an increase in the total pore volume. In the coal sample treated with O 300 I 200, the inorganic and organic molecules are loose. After immersion in water, the pores of the coal sample are dredged, large pores and throughholes fall off, small pores increase, and pore volume ...
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Airdried moisture: Moisture (water) in a sample after airdrying. Airdrying removes surface moisture prior to analysis. Because this term was also sometimes used for residual moisture, it was withdrawn by the American Society for Testing and Materials (ASTM method D12109; American Society for Testing and Materials, 2013, p. 355368).
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SAMPLE PROBLEMS: 2 g of Dried Air Coal sample was taken in Silica Crucible, after heating it in a muffle furnace at 105110°C for 1 hour, the residue was weighted 2 g. The residue was heated in silica crucible covered with vented lid at temperature 950 ± 20°C for exactly 7 minutes. After cooling weight of residue was found to be 1 g.
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Take (±) g (accurate to ) of airdry coal sample in a porcelain boat with a particle size of less than ; and cover the coal sample with a thin layer of tungsten xide. Place the porcelain boat on the quartz tray for sample delivery, start the sampledelivery program controller, and the coal sample shall be
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Method B (air drying method) Method summary Weigh a certain amount of coal sample for general analysis test; place them in blast drying oven at (105 ~ 110) °C; dry them in an air stream to a constant mass. The mass fraction of water is calculated from the mass loss of the coal sample. Instrumentation
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After being soaked in water for 20 days and air dried for 10 days, the coal sample loosened and the chain reaction accelerated. These effects promote the oxidation and spontaneous combustion of coal. Coal samples immersed for 90 days and air dried for 4 days show decreased activation energy and increased tendency for spontaneous combustion.
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1. Moisture content About 1 gm of powdered airdried coal sample is taken in a crusible, and is heated at 100 − 10 5 ∘ C in an electric hotair oven for 1 hour. The loss in weight of the sample is found out and the % of moisture is calculated as % of moisture in coal = weight of airdried coal loss in weight of the coal × 100 2.
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The beginning point and end point should be set in a position which away from the truck 5 meters, and the third point should at the center position. Then digs meters and samples the subsample. That is the manual coal sample method. Workers need to get the sample by the drill.
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The coal is first finely ground and air dried. Samples of the dried coal are then subjected to several operations, with the sample weights being recorded before and after each operation. Moisture content is determined as the weight loss when a sample is held at 105°C in an oxygenfree atmosphere for roughly 2 hours, added to the weight loss ...
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Example 1: You have a set of airdried results where the asanalyzed Moisture is % (ad) and Ash is % (ad). For a contract you are required to report the Ash to a Moisture basis of % basis. 100 Moisture (required basis) . Ash result (ad) = Ash result (at required basis) 100 Moisture (ad) (100 ) . = % (ad) (100 )
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where M ad represents the airdrying base moisture, %; m and m 1 are the coal sample weight and its lost after the drying, g. The equilibrium moisture ( M e ) is defined as the moisture content when the pore water in the coal sample with ∼ mm pores reaches saturation at a temperature of 30°C and a relative humidity of 96% (using a ...
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Drying in a minimum freespace oven at 150 °C (302 °F) within a nitrogen atmosphere Drying in air at 100 to 105 °C (212 to 221 °F) and relative loss of mass determined Methods 1 and 2 are suitable with lowrank coals, but method 3 is only suitable for highrank coals as free air drying lowrank coals may promote oxidation.
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A material supplier from Belgium would like to produce limestone powder for his custome...
India is rich in various mineral resources and it is an important mineral processing market
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