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WhatsApp: +86 18203695377WEBThe best combination is 1 mg of KBr and 99 mg of sample. This ratio I used for large mw (>100 kilo Dalton) samples and for low mw (>350 Dalton) samples as well. I got very nice results. Regards ...
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WhatsApp: +86 18203695377WEBAdd about 1 to 2 percent of your sample, mix and grind to a fine powder. For very hard samples, add the sample first, grind, add KBr and then grind again. The sample must be very finely ground as in the Nujol mulling technique to reduce stering losses and absorption band distortions. Take two stainless steel disks out of the desicor.
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WhatsApp: +86 18203695377WEBThe faults described below are for pure KBr or other halide salts which do not contaminate the sample. When the sample powder is added to the halide salt for pellet making, the clarity of the disc will depend to a large extent on the quantity and type of sample. Usually to 2% weight to weight of sample to KBr is perfectly adequate.
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WhatsApp: +86 18203695377WEBFor measurement of thin film samples with a film thickness of up to 1 µm, the highsensitivity reflection method is widely used, but recently, singlereflection ATR is also being utilized. This article introduces examples of thin film analysis using the highsensitivity reflection and singlereflection ATR methods. 1.
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